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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
922495-54-3
合成路线
（共 8 条）
109-04-6
邻溴吡啶
+
1191060-45-3
→
反应条件
922495-54-3
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in toluene T=110°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
1430731-80-8
+
613-94-5
苯甲酰肼
→
反应条件
922495-54-3
反应条件
1-methyl-pyrrolidin-2-one; potassium carbonate T=70°C; 4 h;
参考文献
Tynebor, Robert; Millings, Elizabeth
Synthetic Communications, 2013 , vol. 43, # 14 p. 1902 - 1908
21510-43-0
2-(4-溴苯基)-5-苯基-1,3,4-恶二唑
→
反应条件
922495-54-3
反应条件
1.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 1.2: 2.75 h / -50 - 20 °C / Inert atmosphere 2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
98-88-4
苯甲酰氯
→
反应条件
922495-54-3
反应条件
1.1: triethylamine 2.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere 3.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 3.2: 2.75 h / -50 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
613-94-5
苯甲酰肼
→
反应条件
922495-54-3
反应条件
1.1: triethylamine / chloroform / 1 h / 20 °C 2.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere 3.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 3.2: 2.75 h / -50 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
6781-60-8
→
反应条件
922495-54-3
反应条件
1.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere 2.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 2.2: 2.75 h / -50 - 20 °C / Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
586-75-4
4-溴苯甲酰氯
→
反应条件
922495-54-3
反应条件
1.1: triethylamine / chloroform / 1 h / 20 °C 2.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere 3.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 3.2: 2.75 h / -50 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
5933-32-4
对溴苯甲酰肼
→
反应条件
922495-54-3
反应条件
1.1: triethylamine 2.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere 3.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere 3.2: 2.75 h / -50 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57
