3,3-二甲氧基氧杂环丁烷合成路线 (共 2 条)
反应条件
Montmorillonite K10 clay in dichloromethane 70 h; Heating;
参考文献
Wuitschik, Georg; Rogers-Evans, Mark; Mueller, Klaus; Fischer, Holger; Wagner, Bjoern; Schuler, Franz; Polonchuk, Liudmila; Carreira, Erick M.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 46 p. 7736 - 7739
反应条件
1: 3,3-dimethoxyoxetane in dichloromethane T=48°C; 72 h; Inert atmosphere; 2: (S)-(-)-2-methyl-2-propanesulfinamide With titanium tetraethoxide in tetrahydrofuran T=50°C; 5 h; Inert atmosphere;
参考文献
Hamzik, Philip J.; Brubaker, Jason D.
Organic Letters, 2010 , vol. 12, # 5 p. 1116 - 1119