反应条件
1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran
Horner-Wadsworth-Emmons olefination; 0.5 h; Inert atmosphere;
2: 2-trans,4-trans-n-heptadienal in tetrahydrofuran
T=-35°C; Horner-Wadsworth-Emmons olefination; 1 h;
参考文献
Kumazawa, Kenji; Sakai, Nao; Amma, Hiroko; Sakamoto, Satoshi; Kodama, Masaki; Wada, Yoshiyuki; Nishimura, Osamu
Bioscience, Biotechnology and Biochemistry, 2010 , vol. 74, # 6 p. 1231 - 1236