10,12-二十五碳二炔-1-醇合成路线 （共 4 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 1.75 h;
参考文献
Morin, Emmanuelle; Guenet, Jean-Michel; Diaz, David D.; Remy, Jean-Serge; Wagner, Alain
Journal of Physical Chemistry B, 2010 , vol. 114, # 39 p. 12495 - 12500
反应条件
1: n-butyllithium, iodine / hexane / 4 h 2: 10percent aq. potassium hydroxide, hydroxylamine hydrochloride, copper(I) chloride, 70percent aq. ethylamine / methanol; tetrahydrofuran / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 1 p. 11 - 14
反应条件
potassium hydroxide; hydroxylamine hydrochloride; ethylamine; copper(l) chloride in tetrahydrofuran; methanol Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 1 p. 11 - 14
反应条件
dibromotriphenyl-phosphorane in acetonitrile
Ambient temperature;
参考文献
Kolotilo, N. V.; Budilova, I. Yu; Bliznyuk, V. N.; Shilov, V. V.; Il'chenko, A. Ya
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 131 - 135
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 156 - 161
