4,5,9-三硫杂十二碳-1,6,11-三烯 9-氧化物合成路线 （共 2 条）
反应条件
trifluoroacetic acid in tetrahydrofuran
T=64°C; 4 h; Product distribution / selectivity;
参考文献
DANMARKS TEKNISKE UNIVERSITET; BJARNSHOLT, Thomas; HOEIBY, Niels; JENSEN, Peter OEstrup; PHIPPS, Richard; SHANMUGHAM, Meenakshi Sundaram; GENNIP, Maria van; CHRISTENSEN, Louise Dahl; JAKOBSEN, Tim Holm; TANNER, David; LARSEN, Thomas Ostenfeld; GIVSKOV, Michael
Patent: WO2012/76016 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
1: 3,3-dimethyldioxirane / acetone / 0.75 h / -50 - -20 °C / Inert atmosphere
2: trifluoroacetic acid / tetrahydrofuran / 4 h / 64 °C
View Scheme
参考文献
DANMARKS TEKNISKE UNIVERSITET; BJARNSHOLT, Thomas; HOEIBY, Niels; JENSEN, Peter OEstrup; PHIPPS, Richard; SHANMUGHAM, Meenakshi Sundaram; GENNIP, Maria van; CHRISTENSEN, Louise Dahl; JAKOBSEN, Tim Holm; TANNER, David; LARSEN, Thomas Ostenfeld; GIVSKOV, Michael
Patent: WO2012/76016 A1, 2012 ;
