N-甲基-4-溴-3-甲基苯磺酰胺合成路线 （共 3 条）
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=80°C;
参考文献
HADIDA RUAH, SARA S.; Miller, Mark; Zhou, Jinglan; Bear, Brian; Grootenhuis, Peter
Patent: US2009/143381 A1, 2009 ;
Location in patent: Page/Page column 56 ;
反应条件
triethylamine in tetrahydrofuran; dichloromethane
T=0°C;
参考文献
Almirall, S.A.; Vidal Juan, Bernat; Gonzalez Rodriguez, Jacob; Gual Roig, Silvia; Esteve Trias, Cristina; Vidal Gispert, Laura
Patent: EP2738172 A1, 2014 ;
Location in patent: Paragraph 0197 ;
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in 1,4-dioxane
T=100°C; Schlenk techniqueInert atmosphere;
参考文献
Almirall, S.A.; Vidal Juan, Bernat; Gonzalez Rodriguez, Jacob; Gual Roig, Silvia; Esteve Trias, Cristina; Vidal Gispert, Laura
Patent: EP2738172 A1, 2014 ;
Location in patent: Paragraph 0108; 0198 ;
