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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
92362-23-7
合成路线
（共 8 条）
542-28-9
delta-戊内酯
+
1119-51-3
5-溴-1-戊烯
→
反应条件
92362-23-7
反应条件
1: 5-bromo-1-pentene With magnesium in tetrahydrofuran T=-78 - 45°C; 2: tetrahydropyran-2-one in tetrahydrofuran T=-78°C; 5 h;
参考文献
Guerinot, Amandine; Serra-Muns, Anna; Gnamm, Christian; Bensoussan, Charlelie; Reymond, Sebastien; Cossy, Janine
Organic Letters, 2010 , vol. 12, # 8 p. 1808 - 1811
56459-15-5
→
反应条件
92362-23-7
反应条件
diisobutylaluminium hydride in dichloromethane T=-78°C; Inert atmosphere;
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
542-28-9
delta-戊内酯
+
34164-50-6
→
反应条件
92362-23-7
+
92362-22-6
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; 4 h;
参考文献
Doherty, Annette M.; Ley, Steven V.; Lygo, Barry; Williams, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 1371 - 1378
1501-26-4
4-氯甲酰基丁酸甲酯
→
反应条件
92362-23-7
反应条件
1: diethyl ether / 0 °C / |Inert atmosphere 2: diisobutylaluminium hydride / dichloromethane / -78 °C / |Inert atmosphere View Scheme
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
34164-50-6
→
反应条件
92362-23-7
反应条件
1: diethyl ether / 0 °C / |Inert atmosphere 2: diisobutylaluminium hydride / dichloromethane / -78 °C / |Inert atmosphere View Scheme
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
111-29-5
1,5-戊二醇
→
反应条件
92362-23-7
反应条件
1.1: sodium hydride / tetrahydrofuran / |Inert atmosphere 1.2: 0 °C / |Inert atmosphere 2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / |Inert atmosphere 3.1: diethyl ether / 0 °C / |Inert atmosphere 4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / |Inert atmosphere 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere View Scheme
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
83067-20-3
5-(叔丁基二甲基硅杂氧基)-1-戊醇
→
反应条件
92362-23-7
反应条件
1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / |Inert atmosphere 2: diethyl ether / 0 °C / |Inert atmosphere 3: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / |Inert atmosphere 4: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere View Scheme
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
87184-80-3
5-((叔丁基二甲基甲硅烷基)氧基)戊醛
→
反应条件
92362-23-7
反应条件
1: diethyl ether / 0 °C / |Inert atmosphere 2: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / |Inert atmosphere 3: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere View Scheme
参考文献
Xie, Youwei; Floreancig, Paul E.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 19 p. 4926 - 4929
Angew. Chem., 2014 , vol. 126, # 19 p. 5026 - 5029,4
