3,3-二甲基丙烯酸甲酯合成路线 （共 110 条）
反应条件
hydrazine hydrate in ethanol
T=20°C; 5 h; Reflux;
参考文献
Gould, Eoin; Lebl, Tomas; Slawin, Alexandra M. Z.; Reid, Mark; Davies, Tony; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7877 - 7892
反应条件
1: AlCl3 / CH2Cl2
2: AcOH; H2SO4
View Scheme
参考文献
Chattapadhyay, Tarun Kumar; Dureja, Prem
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 6 p. 2129 - 2133
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide
1.) THF, -78 deg C, 2.) THF, -78 deg C; Yield given. Multistep reaction;
参考文献
Nishigaichi, Yutaka; Yoshikawa, Miyuki; Takigawa, Yasuyo; Takuwa, Akio
Chemistry Letters, 1996 , # 11 p. 961 - 962
反应条件
1: AlCl3 / CH2Cl2
2: AcOH; H2SO4
View Scheme
参考文献
Chattapadhyay, Tarun Kumar; Dureja, Prem
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 6 p. 2129 - 2133
反应条件
N-bromosuccinmide; dibenzoyl peroxide
参考文献
Martin,R. et al.
Helvetica Chimica Acta, 1976 , vol. 59, # 8 p. 2724 - 2727
Full Text Show Details
Ehrlich,K.; Emerson,G.F.
Journal of the American Chemical Society, 1972 , vol. 94, # 7 p. 2464 - 2470
反应条件
1: AlCl3 / CH2Cl2
2: AcOH; H2SO4
View Scheme
参考文献
Chattapadhyay, Tarun Kumar; Dureja, Prem
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 6 p. 2129 - 2133
反应条件
1: AlCl3 / CH2Cl2
2: AcOH; H2SO4
View Scheme
参考文献
Chattapadhyay, Tarun Kumar; Dureja, Prem
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 6 p. 2129 - 2133
反应条件
in diethyl ether
T=0°C; 1 h;
参考文献
Stavinoha,J.L.; Mariano,P.S.; Leone-Bay,A.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3148
参考文献
Wagner
Journal of the American Chemical Society, 1949 , vol. 71, p. 3216
反应条件
1: (i) LDA*HMPT, THF, (ii) /BRN= 1071199/
2: LDA*HMPT / tetrahydrofuran
3: aq. NaOH, MeOH
View Scheme
参考文献
Brocksom,T.J. et al.
Synthetic Communications, 1977 , vol. 7, p. 483 - 493
