3,3-二甲基丙烯酸甲酯合成路线 （共 110 条）
反应条件
diethyl ether anfangs unter Kuehlung;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3216
参考文献
Journal of the American Chemical Society, , vol. 110, p. 1880
反应条件
1: 65 percent / triethylamine / dimethylformamide / 48 h / Heating 2: 90 percent / SCl2 / various solvent(s); CCl4 / 0.25 h / 40 °C 3: various solvent(s); CCl4 / 1.5 h / Heating 4: 97 percent / CH2Cl2 / 4 h / Ambient temperature 5: 90 percent / NaOH / hexane; H2O 6: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 7: 28 percent / methanol / 3 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4429 - 4439
反应条件
1: 100 percent / bromine / CHCl3 / 2 h / Heating 2: 73 percent / Na2S / methanol / 2 h 3: 97 percent / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / NaOH / hexane; H2O 5: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 6: 28 percent / methanol / 3 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4429 - 4439
反应条件
1: 90 percent / SCl2 / various solvent(s); CCl4 / 0.25 h / 40 °C 2: various solvent(s); CCl4 / 1.5 h / Heating 3: 97 percent / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / NaOH / hexane; H2O 5: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 6: 28 percent / methanol / 3 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4429 - 4439
反应条件
1: various solvent(s); CCl4 / 1.5 h / Heating 2: 97 percent / CH2Cl2 / 4 h / Ambient temperature 3: 90 percent / NaOH / hexane; H2O 4: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 5: 28 percent / methanol / 3 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4429 - 4439
反应条件
1: 90 percent / NaOH / hexane; H2O 2: 100 percent / 2,2,4-trimethyl-pentane / 0.25 h / Heating 3: 28 percent / methanol / 3 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4429 - 4439
反应条件
1: dimethyl methoxycarbonylmethanephosphonate With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.5 h; Inert atmosphere; 2: acetone in tetrahydrofuran; mineral oil T=0 - 20°C; Horner-Wittig reaction; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 23 p. 8319 - 8321
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3216
反应条件
in methanol Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4804 - 4805
