3-溴呋喃并[2,3-c]吡啶合成路线 (共 6 条)
反应条件
methyl lithium LiBr complex; water 1.) THF, ether, -75 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 413 - 422
反应条件
n-butyllithium; N,N-dimethyl-formamide 1.) THF, hexane, -75 deg C, 30 min, 2.) THF, hexane, a.) -75 deg C, 1 h, b.) -30 deg C, 1 h, c.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 413 - 422
反应条件
1.) THF, hexane, -75 deg C, 30 min, 2.) THF, hexane, a.) -75 deg C, 1 h, b.) -30 deg C, 1 h, c.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 413 - 422
反应条件
methyl lithium LiBr complex; water 1.) THF, ether, -75 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 413 - 422
反应条件
sodium hydroxide in methanol; water
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Heterocycles, 1984 , vol. 21, # 2 p. 738
反应条件
bromine in chloroform
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki; Inoue, Masatoshi; Ishida, Toshimasa; Iitaka, Yoichi; Itai, Akiko
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 725 - 736