5-氨基-1-甲基-1H-吡唑-3-羧酸甲酯合成路线 （共 8 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol P=38002.6 Torr; 1 h;
参考文献
KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
Patent: US2010/63106 A1, 2010 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen; palladium 10 on activated carbon in ethanol P=1551.49 Torr; 16 h;
参考文献
WO2004/98589 A1, ;
Page 166 ;
WO 2004/098589 A1
反应条件
in methanol T=18 - 25°C; 48 h;
参考文献
US2011/275628 A1, ;
Page/Page column 18 ;
反应条件
hydrogen; palladium on activated charcoal P=2660 Torr; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: 89 percent / KOH / methanol / 24 h / 20 °C 2: SOCl2 / 0.5 h / Heating 3: NaN3 / acetone; H2O / 0.02 h 4: toluene / 0.5 h / Heating 5: H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: NaN3 / acetone; H2O / 0.02 h 2: toluene / 0.5 h / Heating 3: H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: SOCl2 / 0.5 h / Heating 2: NaN3 / acetone; H2O / 0.02 h 3: toluene / 0.5 h / Heating 4: H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
72 h; Ambient temperature;
参考文献
Adachi; Yamamori; Hiramatsu; Sakai; Sato; Kawakami; Uno; Ueda
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 8 p. 3235 - 3252
