3,4,6-三邻乙酰基-alpha-D-吡喃葡萄糖 1,2-(原酸甲酯)合成路线 （共 22 条）
反应条件
1.1: 99 percent / Bu3SnOMe / 1,2-dichloro-ethane / 2 h / 90 °C
2.1: K2CO3; molecular sieves 3A / CH2Cl2 / 0.42 h / 0 °C
2.2: 75 percent / CH2Cl2 / 2 h / 0 °C
View Scheme
参考文献
Nakajima, Rika; Ono, Machiko; Aiso, Sadakazu; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 6 p. 684 - 687
反应条件
1.1: 60 percent / Bu3SnOMe / 1,2-dichloro-ethane / 5 h / 90 °C
2.1: K2CO3; molecular sieves 3A / CH2Cl2 / 0.42 h / 0 °C
2.2: 75 percent / CH2Cl2 / 2 h / 0 °C
View Scheme
参考文献
Nakajima, Rika; Ono, Machiko; Aiso, Sadakazu; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 6 p. 684 - 687
