反应条件
1: CHIRALPAK AD-H column / |Resolution of racemate 2: 1H-imidazole / dichloromethane / 16 h / 0 - 5 °C 3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 55 °C 4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 25 °C View Scheme
参考文献
Shoup, Timothy M.; McCauley, John P.; Lee Jr., David F.; Chen, Rui; Normandin, Marc D.; Bonab, Ali A.; El Fakhri, Georges; Vasdev, Neil
Tetrahedron Letters, 2014 , vol. 55, # 3 p. 682 - 685
