N-苄基-N-甲氧基-2,3-丙烯胺合成路线 （共 4 条）
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate T=0 - 10°C; 0.5 h; 2: 1-(N-acetyl-N-benzylamino)propene T=10 - 90°C; 7 h; Product distribution / selectivity;
参考文献
Council of Scientific and Industrial Research
Patent: EP1348699 A1, 2003 ;
Location in patent: Page/Page column 2-3 ;
反应条件
trichlorophosphate 1.) 2 h, room temperature, 2.) 4 h, 75 deg C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 6 p. 1173 - 1182
反应条件
triethylamine in benzene
1.) 5-8 deg C, 2.) room temperature, 1 h;
参考文献
Meth-Cohn, Otto; Westwood, Keith T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 6 p. 1173 - 1182
反应条件
1: 83 percent / KOH / 1.) 5-8 deg C, 2 h, 2.) room temperature, 30 min
2: 61 percent / Et3N / benzene / 1.) 5-8 deg C, 2.) room temperature, 1 h
View Scheme
参考文献
Meth-Cohn, Otto; Westwood, Keith T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 6 p. 1173 - 1182
