肼基甲酸-o-叔丁基-n-4-硝基苯酯合成路线 （共 13 条）
反应条件
1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 2: trichloromonobromomethane; trifluoroacetic acid / benzene / 20 °C View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 2: trifluoroacetic acid / acetonitrile / 80 °C View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 2: iodine; trifluoroacetic acid / acetonitrile / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 77, # 3 p. 1520 - 1532
反应条件
1.1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 2.1: oxygen; trifluoroacetic acid / acetonitrile / 60 °C / 760.05 Torr 2.2: 20 °C View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere 2: manganese(IV) oxide; trifluoroacetic acid; copper dichloride / acetonitrile / 80 °C View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
in acetonitrile
7 h; Heating;
参考文献
Kisseljova, Ksenija; Tsubrik, Olga; Sillard, Rannar; Maeeorg, Sirje; Maeeorg, Uno
Organic Letters, 2006 , vol. 8, # 1 p. 43 - 45
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=10 - 20°C; 16 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
lauryl mercaptan in dimethyl sulfoxide
参考文献
Hoefling, Sarah B.; Bartuschat, Amelie L.; Heinrich, Markus R.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 50 p. 9769 - 9772
反应条件
1: 4-methyl-morpholine / dichloromethane / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 10 - 20 °C
View Scheme
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
1: hydroxylamine; sodium hydrogencarbonate / methanol; water
2: 4-methyl-morpholine / dichloromethane / 0 - 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 10 - 20 °C
View Scheme
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
