肼基甲酸-o-叔丁基-n-4-硝基苯酯合成路线 （共 13 条）
参考文献
Carpino,L.A. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4336 - 4340
反应条件
1.1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere
2.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: trifluoroacetic acid / acetonitrile / 80 °C
4.1: trichloromonobromomethane; trifluoroacetic acid / acetonitrile / 80 °C
View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
反应条件
1.1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere
2.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: iodine; trifluoroacetic acid / acetonitrile / 80 °C
View Scheme
参考文献
Jasch, Hannelore; Hoefling, Sarah B.; Heinrich, Markus R.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1520 - 1532
