4-甲氧基-2-甲基-联苯合成路线 （共 109 条）
反应条件
potassium carbonate; palladium diacetate in water; acetone
T=65°C; 16 h;
参考文献
Wallow, Thomas I.; Novak, Bruce M.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 5034 - 5037
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran
T=0°C; 0.5 h;
2: 1-bromo-2-methyl benzene in tetrahydrofuran
T=0 - 25°C; 24 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran
T=60°C; Arylation; 36 h;
参考文献
Hirabayashi, Kazunori; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Organic Letters, 1999 , vol. 1, # 2 p. 299 - 301
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide
T=80°C; 3 h;
参考文献
Nakao, Yoshiaki; Oda, Takuro; Sahoo, K. Akhila; Hiyama, Tamejiro
Journal of Organometallic Chemistry, 2003 , vol. 687, # 2 p. 570 - 573
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II)
T=80°C; Hiyama cross-coupling reaction; 2 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Xie, Ye-Xiang
Synthesis, 2006 , # 6 p. 969 - 974
反应条件
1: 1-chloro-1-(4'-methoxyphenyl)silacyclobutane With tetrabutyl ammonium fluoride in tetrahydrofuran
2: 1-iodo-2-methylbenzene With tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran
3 h; Heating; Further stages.;
参考文献
Denmark, Scott E.; Wu, Zhicai
Organic Letters, 1999 , vol. 1, # 9 p. 1495 - 1498
反应条件
tetrabutylammomium bromide; palladium diacetate in tetrahydrofuran
T=20°C; Negishi coupling; 4 h; Inert atmosphere;
参考文献
Liu, Jing; Deng, Yi; Wang, Haibo; Zhang, Hua; Yu, Ganxiang; Wu, Bingbin; Zhang, Heng; Li, Qiang; Marder, Todd B.; Yang, Zhen; Lei, Aiwen
Organic Letters, 2008 , vol. 10, # 13 p. 2661 - 2664
反应条件
bathophenanthroline; potassium tert-butylate; ferrous acetate
T=20 - 80°C; Inert atmosphere;
参考文献
Vallee, Frederic; Mousseau, James J.; Charette, Andre B.
Journal of the American Chemical Society, 2010 , vol. 132, # 5 p. 1514 - 1516
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=20°C; 4 h; Inert atmosphere;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2010 , vol. 12, # 19 p. 4388 - 4391
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide; sodium hydroxide in water
T=60°C; Hiyama coupling; 10 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Chemical Communications, 2010 , vol. 46, # 47 p. 9046 - 9048
