2,2'-硫代二乙酸二乙酯合成路线 （共 25 条）
反应条件
hydrogenchloride; ethanol
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 85, p. 567 - 579
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 955 - 961
反应条件
sodium ethanolate Abdampfen der mit Wasser versetzten Mischung und Ansaeuern mit Salzsaeure;
参考文献
Hinsberg
Chemische Berichte, 1912 , vol. 45, p. 2417
反应条件
ethanol; sodium ethanolate T=20°C; 3.5 h; Reflux;
参考文献
Zhang, Hua; Qian, Chao; Chen, Xin-Zhi
Journal of Chemical Research, 2011 , vol. 35, # 6 p. 339 - 340
反应条件
sodium methylate in methanol T=20°C; 72 h;
参考文献
Henckens; Colladet; Fourier; Cleij; Lutsen; Gelan; Vanderzande
Macromolecules, 2005 , vol. 38, # 1 p. 19 - 26
反应条件
selenium(IV) oxide; dihydrogen peroxide in methanol T=20°C; 0.2 h;
参考文献
Edayadulla, Naushad; Ramesh, Penugonda
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 2056 - 2063
反应条件
1.1: NaOEt / ethanol / 0.5 h 1.2: 66 percent / ethanol / 18 h / Heating 2.1: 43 percent / DEAD; Ph3P / tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Far Eastern New Century Corporation; Liang, Nai-Yun; Tsai, Hui-Shan; Ke, Ching-Wei; Jseng, Chin-Wan
Patent: EP2548875 A1, 2013 ;
参考文献
Solladie-Cavallo,A.; Vieles,P.
Bulletin de la Societe Chimique de France, 1967 , p. 517 - 523
反应条件
sodium ethanolate in ethanol T=68°C; 1 h; Microwave irradiation; WavelengthTime;
参考文献
Far Eastern New Century Corporation; Liang, Nai-Yun; Tsai, Hui-Shan; Ke, Ching-Wei; Jseng, Chin-Wan
Patent: EP2548875 A1, 2013 ;
Location in patent: Paragraph 0074-0082 ;
反应条件
1: thiodiacetic acid diethyl ester; 1,2-dichloro-ethane; oxalic acid diethyl ester With potassium methanolate in methanol T=0 - 40°C; 5 h; Heating / reflux; 2: With sodium hydrogen sulphate in methanol 0.166667 h; 3: 1,2-dichloro-ethane With sodium hydroxide; potassium carbonate more than 3 stages;
参考文献
Bayer Aktiengesellschaft
Patent: EP1167368 A1, 2002 ;
Location in patent: Page 5-6 ;
