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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
925211-06-9
合成路线
（共 24 条）
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
128946-78-1
(1R,5S)-3-氧杂二环[3.3.0]辛-6-烯-2-酮
+
103618-27-5
反应条件
ethylenediaminetetraacetic acid; oxygen; Adenine-flavine dinucleotide; NADP in water T=30°C; Baeyer-Villiger oxidation reaction; pH=7.4; Irradiationkinetic resolution;
参考文献
Jensen, Chantel N.; Cartwright, Jared; Ward, Jonathan; Hart, Sam; Turkenburg, Johan P.; Ali, Sohail T.; Allen, Michael J.; Grogan, Gideon
ChemBioChem, 2012 , vol. 13, # 6 p. 872 - 878
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
128946-78-1
(1R,5S)-3-氧杂二环[3.3.0]辛-6-烯-2-酮
反应条件
(1S,2S)-trans-1,2-cyclohexanediol in ethanol T=25°C; 5 h; Acinetobacter TD63;
参考文献
Journal of Organic Chemistry, , vol. 57, # 4 p. 1306 - 1309
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
反应条件
Co(lll)(Salen); triton X-114; dihydrogen peroxide in water T=5°C; Baeyer-Villiger oxidation; 24 h; enantioselective reaction;
参考文献
Bianchini, Giulio; Cavarzan, Alessandra; Scarso, Alessandro; Strukul, Giorgio
Green Chemistry, 2009 , vol. 11, # 10 p. 1517 - 1520
925211-06-9
→
反应条件
71155-04-9
双环[3.2.0]庚-2-烯-6-酮
+
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
71155-05-0
双环[3.2.0]庚-2-烯-6-酮
+
103618-27-5
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; {(4R,5R)-5-[(hydroperoxydiphenyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}diphenylmethanol in tetrahydrofuran T=-30°C; 1 h; Further byproducts given;
参考文献
Aoki, Masao; Seebach, Dieter
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 187 - 207
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
71155-05-0
双环[3.2.0]庚-2-烯-6-酮
+
103618-27-5
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; {(4R,5R)-5-[(hydroperoxydiphenyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}diphenylmethanol in tetrahydrofuran T=-30°C; Baeyer-Villiger oxidation; 1 h; Further byproducts given;
参考文献
Aoki, Masao; Seebach, Dieter
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 187 - 207
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
128946-78-1
(1R,5S)-3-氧杂二环[3.3.0]辛-6-烯-2-酮
+
103618-27-5
反应条件
ethylenediaminetetraacetic acid; oxygen; Adenine-flavine dinucleotide; NADP in water T=30°C; Baeyer-Villiger oxidation reaction; pH=7.4; Irradiationkinetic resolution;
参考文献
Jensen, Chantel N.; Cartwright, Jared; Ward, Jonathan; Hart, Sam; Turkenburg, Johan P.; Ali, Sohail T.; Allen, Michael J.; Grogan, Gideon
ChemBioChem, 2012 , vol. 13, # 6 p. 872 - 878
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
128946-78-1
(1R,5S)-3-氧杂二环[3.3.0]辛-6-烯-2-酮
反应条件
(1S,2S)-trans-1,2-cyclohexanediol in ethanol T=25°C; 5 h; Acinetobacter TD63;
参考文献
Alphand, Veronique; Furstoss, Roland
Journal of Organic Chemistry, 1992 , vol. 57, # 4 p. 1306 - 1309
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
反应条件
Co(lll)(Salen); triton X-114; dihydrogen peroxide in water T=5°C; Baeyer-Villiger oxidation; 24 h; enantioselective reaction;
参考文献
Bianchini, Giulio; Cavarzan, Alessandra; Scarso, Alessandro; Strukul, Giorgio
Green Chemistry, 2009 , vol. 11, # 10 p. 1517 - 1520
925211-06-9
→
反应条件
71155-04-9
双环[3.2.0]庚-2-烯-6-酮
+
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
71155-05-0
双环[3.2.0]庚-2-烯-6-酮
+
103618-27-5
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; {(4R,5R)-5-[(hydroperoxydiphenyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}diphenylmethanol in tetrahydrofuran T=-30°C; 1 h; Further byproducts given;
参考文献
Aoki, Masao; Seebach, Dieter
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 187 - 207
925211-06-9
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
71155-05-0
双环[3.2.0]庚-2-烯-6-酮
+
103618-27-5
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; {(4R,5R)-5-[(hydroperoxydiphenyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}diphenylmethanol in tetrahydrofuran T=-30°C; Baeyer-Villiger oxidation; 1 h; Further byproducts given;
参考文献
Aoki, Masao; Seebach, Dieter
Helvetica Chimica Acta, 2001 , vol. 84, # 1 p. 187 - 207
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