1-甲基-5-三甲基锡-1H-吡唑合成路线 （共 5 条）
反应条件
cesium fluoride in N,N-dimethyl-formamide T=50°C; 1.33333 h;
参考文献
Journal of Organic Chemistry, , vol. 49, # 24 p. 4687 - 4695
反应条件
potassium carbonate in acetone
T=40°C; 92 h;
参考文献
Effenberger, Franz; Krebs, Andreas
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4687 - 4695
反应条件
n-butyllithium
1. hexane, ether, 3 h, -30 deg C 2. -30 deg C -> room temp., overnight; Yield given. Multistep reaction;
参考文献
Effenberger, Franz; Krebs, Andreas
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4687 - 4695
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine
1. hexane, ether, 3 h, -30 deg C 2. -30 deg C -> room temp., overnight; Yield given. Multistep reaction;
参考文献
Effenberger, Franz; Krebs, Andreas
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4687 - 4695
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=50°C; 20 h;
参考文献
Effenberger, Franz; Krebs, Andreas
Journal of Organic Chemistry, 1984 , vol. 49, # 24 p. 4687 - 4695
