4-甲基-1,3-戊二烯合成路线 (共 99 条)
反应条件
potassium hydroxide; copper dichloride
参考文献
Mariano, Patrick S.; Bay, Elliott; Watson, Darrell G.; Rose, Timothy; Bracken, Christopher
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1753 - 1762
反应条件
iodo-alcohol; silver nitrate
参考文献
Deux
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1943 , vol. 216, p. 416
反应条件
hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; (R,S)-binaphos in benzene
T=30°C; P=76000 Torr; 96 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiuchi, Toshihide; Ohta, Tetsuo; Shirakawa, Eiji; Nozaki, Kyoko; Takaya, Hidemasa
Tetrahedron, 1997 , vol. 53, # 23 p. 7795 - 7804
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
反应条件
hydrogen; potassium cyanide; potassium hydroxide; potassium chloride; β-cyclodextrin; cobalt(II) chloride in benzene
P=760 Torr; 50 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Lee, Jong-Tae; Alper, Howard
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1854 - 1856
反应条件
hydrogen; lt;Co(SCN)(PPh3)3gt; in ethylene glycol dimethyl ether
T=17°C; P=760 Torr; relative rate; rate of H2 uptake;; Product distributionMechanism;
参考文献
Nakayama; Kanai
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 16 - 22
反应条件
T=25°C; P=2942.03 Torr; Hydrogenation;
参考文献
Bachman; Hatton
Journal of the American Chemical Society, 1944 , vol. 66, p. 1513
参考文献
Lewina et al.
Sb. Statei Obshch. Khim., 1953 , p. 355,359
Chem.Abstr., 1955 , p. 829
反应条件
potassium tert-butylate
T=-10°C; Yield given. Yields of byproduct given;
参考文献
Holm, Kjetil H.; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 9 p. 783 - 794
反应条件
zinc; trichlorophosphate in diethyl ether
12 h; Ambient temperature;
参考文献
Brady, William T.; Norton, Scott J.; Ko, Jinren
Synthesis, 1983 , # 12 p. 1002 - 1005