Huston; Bostwick
Journal of Organic Chemistry, 1948 , vol. 13, p. 334
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Malinowski; Wolkowa; Morosowa
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 117
methanesulfonic acid in tetrahydrofuran dropwise addn. of i-BuMgBr (2 equiv.) to soln. of C6H11B(OCH(CH3)2)2 (2.5 mmol) in THF at -78°C via syringe; stirring at -78°C for 3 h; addn. of CH3SO3H at -78°C; warming slowly to room temp.; stirring at room temp.;; not isolated; product distribution is determined by 11B-NMR;;
参考文献
Brown, Herbert C.; Vasumathi, Nagarajan; Joshi, Navalkishore N.
Organometallics, 1993 , vol. 12, p. 1058 - 1067
