N2-(2-甲氧基乙基)-2,5-吡啶二胺合成路线 （共 3 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate
T=20°C; 16 h;
参考文献
Gruenenthal GmbH; FRANK, Robert; Christoph, Thomas; Lesch, Bernhard; Lee, Jeewoo
Patent: US2013/29961 A1, 2013 ;
Location in patent: Paragraph 0727 ;
反应条件
1: 1 h / 20 °C
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C
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参考文献
GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: WO2013/13817 A1, 2013 ;
WO 2013/013817 A1
反应条件
1: trichlorophosphate; phosphorus pentachloride / 16 h / 60 °C
2: 1 h / 23 °C
3: palladium 10 on activated carbon; hydrogen / ethyl acetate / 16 h / 23 °C
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参考文献
GRÜNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard
Patent: WO2013/13815 A1, 2013 ;
WO 2013/013815 A1
