1: With potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; 0.5 h; Inert atmosphere; 2: With oxygen in tetrahydrofuran; toluene T=-78°C; 3: With hydrogenchloride in water T=20°C; pH=1.2;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449
1: (phenylsulfonyl)methane With potassium hydride in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
2: 1-bromo-3-phenyl-propane in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449