反应条件
1: TsOH / benzene / 72 h / 80 °C
2: LiAlH4 / tetrahydrofuran / 2 h
3: Me3SiCl, NaI / acetonitrile / 0.5 h
4: benzene / 5 h / 80 °C
5: BF3*Et2O / CH2Cl2 / 15 h
7: DCC, DMAP / CH2Cl2 / 72 h
8: 10percent HCl / tetrahydrofuran / 4 h / 50 °C
9: PCC-Al2O3 / CH2Cl2 / 8 h
10: 48percent HF / acetonitrile / 6 h / 50 °C
View Scheme
参考文献
Falck; Yang
Tetrahedron Letters, 1984 , vol. 25, # 33 p. 3563 - 3566
