反式-2-已烯-1-醇合成路线 （共 129 条）
反应条件
in dichloromethane; pentane
参考文献
Eli Lilly and Company
Patent: US5612360 A1, 1997 ;
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent)
T=20 - 25°C; 12 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
benzoic trifluoromethanesulfonic anhydride in acetonitrile
T=20°C; 22 h;
参考文献
Dumeunier, Raphael; Marko, Istvan E.
Tetrahedron Letters, 2004 , vol. 45, # 4 p. 825 - 829
反应条件
3: 65 percent / t-BuSH / benzene / Heating
View Scheme
参考文献
Beckwith, Athelstan L. J.; Davison, G. E.
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 49 - 52
反应条件
bis(acetylacetonato) palladium; triphenylphosphine
T=85 - 90°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
反应条件
propionic acid
T=120°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Daub, G. WIlliam; Lunt, Sharon R.
Tetrahedron Letters, 1983 , vol. 24, # 41 p. 4397 - 4400
反应条件
sodium hydride
5 h; Ambient temperature;
参考文献
Ueno, Yoshio; Khare, R. K.; Okawara, Makoto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2637 - 2640
反应条件
[{nBu4N}5{PV2Mo10O40}]; Nitrous oxide in benzonitrile
T=150°C; P=760 Torr; 15 h;
参考文献
Delaby; Guillot-Allegre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1931 , vol. 192, p. 1468
Bulletin de la Societe Chimique de France, 1933 , vol. <4>53, p. 304,308
反应条件
platinum (II) chloride in dichloromethane
T=20°C; 20 h;
参考文献
Lester, Roy P.; Dunsford, Jay J.; Camp, Jason E.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7472 - 7476
反应条件
1: 1.) NAH / 1.) THF, 0 deg C, 1 h, 2.) THF, RT, 1.5 h
2: decahydronaphthalene / 12 h / Heating
View Scheme
参考文献
Cardillo; Orena; Sandri
Journal of Organic Chemistry, 1986 , vol. 51, # 5 p. 713 - 717
