反应条件
1.1: 50 percent / hydrogen / Pd/C / ethanol / 15 h / 60 °C / 3040 Torr 2.1: HCl; sodium nitrite / H2O / 3.5 h / cooling 2.2: 60 percent / sodium azide / H2O; diethyl ether / 2 h / 0 °C 3.1: 96 percent / hydrazine hydrate / ethanol; tetrahydrofuran; H2O / 26 h / 20 °C 4.1: 33 percent / ethanol / 24 h / Heating View Scheme
参考文献
Wallace, Jeffery M.; Soederberg, Bjoern C. G.; Hubbard, Jeremiah W.
Synthetic Communications, 2006 , vol. 36, # 22 p. 3425 - 3439
