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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
928642-45-9
合成路线
(共 11 条)
928642-45-9
+
615-41-8
1-氯-2-碘苯
→
反应条件
53824-24-1
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 7 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
184368-89-6
→
反应条件
1806-29-7
2,2'-二羟基联苯
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 36 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
625-99-0
1-氯-3-碘苯
→
反应条件
249291-09-6
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 10 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
591-50-4
碘苯
→
反应条件
90-43-7
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 5 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
624-31-7
4-碘甲苯
→
反应条件
101043-55-4
4'-甲基-2-联苯醇
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 26 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
25245-27-6
3,5-二甲氧基碘苯
→
反应条件
168301-25-5
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 5 h; Inert atmosphere; SolventReagent/catalyst;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
610-97-9
2-碘苯甲酸甲酯
→
反应条件
2005-10-9
苯并[c]苯并吡喃-6-酮
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 4 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
609-73-4
2-硝基碘苯
→
反应条件
20281-21-4
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 6 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
696-62-8
4-碘苯甲醚
→
反应条件
21849-91-2
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 32 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
928642-45-9
+
74497-02-2
→
反应条件
644-71-3
2-苯胺基苯酚
反应条件
oxygen; copper diacetate in 1,4-dioxane T=80°C; 3 h; Schlenk techniqueSealed tube; Catalytic behavior; Solvent;
参考文献
Ding, Dong; Lv, Xiaobing; Li, Jian; Xu, Guangyang; Ma, Bing; Sun, Jiangtao
Chemistry - An Asian Journal, 2014 , vol. 9, # 6 p. 1539 - 1542
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