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乙二醇
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63148-62-9
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4-异恶唑硼酸频哪醇酯
合成路线
(共 22 条)
928664-98-6
4-异恶唑硼酸频哪醇酯
+
5111-65-9
2-溴-6-甲氧基萘
→
反应条件
71056-96-7
2-(6-甲氧基萘-2-基)乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
612-55-5
2-碘萘
→
反应条件
7498-57-9
2-萘乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
580-13-2
2-溴代萘
→
反应条件
7498-57-9
2-萘乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
3857-83-8
2-萘基三氟甲烷磺酸
→
反应条件
7498-57-9
2-萘乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
580-13-2
2-溴代萘
→
反应条件
7498-57-9
2-萘乙腈
反应条件
bis-triphenylphosphine-palladium(II) chloride; water; sodium carbonate in propan-1-ol T=130°C; Domino Suzuki coupling and fragmentation reaction; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Journal of the American Chemical Society, , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
91-58-7
2-氯萘
→
反应条件
7498-57-9
2-萘乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
99-90-1
4-溴苯乙酮
→
反应条件
10266-42-9
2-(4-乙酰基苯基)乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
95-46-5
邻溴甲苯
→
反应条件
22364-68-7
邻甲基苯乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
402-43-7
对溴三氟甲苯
→
反应条件
2338-75-2
对三氟甲基苯乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
928664-98-6
4-异恶唑硼酸频哪醇酯
+
580-13-2
2-溴代萘
→
反应条件
7498-57-9
2-萘乙腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
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