1,8-二氨基-3,6-二氧杂辛烷合成路线 （共 65 条）
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Lee, Jiseok; Kim, Hyong-Jun; Kim, Jinsang
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5010 - 5011
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=0 - 20°C; 9 h;
参考文献
Niikura, Kenichi; Kamitani, Ryosuke; Kurogochi, Masaki; Uematsu, Rie; Shinohara, Yasuro; Nakagawa, Hiroaki; Deguchi, Kisaburo; Monde, Kenji; Kondo, Hirosato; Nishimura, Shin-Ichiro
Chemistry - A European Journal, 2005 , vol. 11, # 13 p. 3825 - 3834
反应条件
1: 75 percent / methanol / 168 h / 25 °C / 750.06 Torr 2: 75 percent / lithium aluminium hydride (LAH) / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Jong, F. de; Zon, A. van; Reinhoudt, D. N.; Torny, G. J.; Tomassen, H. P. M.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 3 p. 164 - 173
反应条件
sodium carbonate in acetonitrile 3 h; Heating;
参考文献
Kulstad, S.; Malmsten, L. A.
Tetrahedron, 1980 , vol. 36, # 4 p. 521 - 524
反应条件
sodium carbonate in acetonitrile 168 h; Heating;
参考文献
Krakowiak; Bradshaw
Tetrahedron Letters, 1993 , vol. 34, # 5 p. 777 - 778
反应条件
2: LiAlH4 3: Et3N 4: B2H6 5: (i) aq. HCl, (ii) ion-exchange resin <OH- form> View Scheme
参考文献
Dietrich,B. et al.
Tetrahedron, 1973 , vol. 29, p. 1629 - 1645
参考文献
Banbery, Hilary J.; McQuillan, Ferida; Hamor, Thomas A.; Jones, Christopher J.; McCleverty, Jon A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1405 - 1408
反应条件
potassium carbonate in acetonitrile
48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
1: ethanol / 168 h / Heating
2: 49 percent / LiAlH4 / tetrahydrofuran / Heating
3: 84 percent / methanol / 6 h / 100 °C / 2250.2 Torr
View Scheme
参考文献
Kulstad,S.; Malmsten,L.A.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1979 , vol. 33, p. 469 - 474
反应条件
1: Na2CO3 / acetonitrile
2: Et3N / ethanol
View Scheme
参考文献
Kulstad,S.; Malmsten,L.A.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1979 , vol. 33, p. 469 - 474
