3,6,9-三氧杂十一烷-1,11-二胺合成路线 （共 26 条）
参考文献
Bogatskii, A.V.; Luk'yanenko, N. G.; Kirichenko, T. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1301 - 1307
反应条件
1: benzene / Heating
2: benzene / 1 h / Heating
3: aq.H2SO4 (96 percent) / 1 h / Heating
View Scheme
参考文献
Bogat-skii, A.V.; Luk'yanenko, N.G.; Shapkin, V.A.; Popkov, Yu.A.; Nazarova, N.Yu.; Chernotkach, Z.A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 798 - 804
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 4 p. 878 - 885
反应条件
triethylamine in benzene
24 h;
参考文献
Luk'yanenko, N. G.; Bogat-skii, A. V.; Shapkin, V. A.; Popkov, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 944 - 950
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1069 - 1077
反应条件
triethylamine in benzene
24 h;
参考文献
Luk'yanenko, N. G.; Bogat-skii, A. V.; Shapkin, V. A.; Popkov, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 944 - 950
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1069 - 1077
反应条件
1: acetonitrile / 20 °C
2: N-ethyl-N,N-diisopropylamine / acetonitrile; water / pH 8 - 9
View Scheme
参考文献
Lindner, Simon; Michler, Christina; Leidner, Stephanie; Rensch, Christian; Waengler, Carmen; Schirrmacher, Ralf; Bartenstein, Peter; Waengler, Bjoern
Bioconjugate Chemistry, 2014 , vol. 25, # 4 p. 738 - 749
反应条件
1.1: triethylamine / toluene / 7 h
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 7 h / Cooling with ice; Reflux
2.2: pH 10
View Scheme
参考文献
Nguyen, Tam; Buckley, Christopher M.; Ellis, Trevor K.; Smith, Gary L. N.; Powell, Douglas R.; Taylor, Richard W.
Journal of Chemical Crystallography, 2012 , vol. 42, # 6 p. 573 - 577
