反应条件
1.1: NaClO2; NaH2PO4; H2O2 / acetonitrile; H2O / 12 h
2.1: toluene; methanol / 0.08 h / 0 °C
3.1: pyridine / 15 h / 40 °C
3.2: trifluoroacetic anhydride / 48 h / 20 °C
3.3: SmI2 / tetrahydrofuran; methanol / 0.5 h / 20 °C
4.1: aq. HCl / 48 h / Heating
4.2: propylene oxide / ethanol / 0.5 h / 60 °C
View Scheme
参考文献
Baumann, Thomas; Vogt, Henning; Braese, Stefan
European Journal of Organic Chemistry, 2007 , # 2 p. 266 - 282
