1: Et3N / diethyl ether / 20 °C
2: SO2Cl2 / diethyl ether / 1 h / 20 °C
3: HCl / 20 h / 38 - 40 °C
View Scheme
参考文献
Turhanen, Petri A.; Demadis, Konstantinos D.; Peraeniemi, Sirpa; Vepsaelaeinen, Jouko J.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1468 - 1471
1.1: Et3N / diethyl ether / 20 °C
2.1: SO2Cl2 / diethyl ether / 1 h / 20 °C
3.1: 100 percent / NaHCO3 / H2O / 1 h / 20 °C
4.1: Me3SiBr; NaHCO3 / acetonitrile / 2 h / 20 °C
4.2: MeOH / acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Turhanen, Petri A.; Demadis, Konstantinos D.; Peraeniemi, Sirpa; Vepsaelaeinen, Jouko J.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1468 - 1471
