hydrogenchloride
T=38 - 40°C; 20 h; Title compound not separated from byproducts;
参考文献
Turhanen, Petri A.; Demadis, Konstantinos D.; Peraeniemi, Sirpa; Vepsaelaeinen, Jouko J.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1468 - 1471
1.1: 100 percent / NaHCO3 / H2O / 1 h / 20 °C
2.1: Me3SiBr; NaHCO3 / acetonitrile / 2 h / 20 °C
2.2: MeOH / acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Turhanen, Petri A.; Demadis, Konstantinos D.; Peraeniemi, Sirpa; Vepsaelaeinen, Jouko J.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1468 - 1471