9-苯基-1,7-二氮杂双环[4.3.0]壬-2,4,6,8-四烯合成路线 （共 22 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane in water
T=60 - 70°C; 1 h; Green chemistry; regioselective reaction;
参考文献
Bangade, Vikas M.; Reddy, B. Chennakesava; Thakur, Pramod B.; Madhu Babu; Meshram
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4767 - 4771
反应条件
oxygen; palladium diacetate; silver carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl-formamide
T=130°C; 20 h; Reagent/catalystSolvent; regioselective reaction;
参考文献
Wang, Shaohua; Liu, Wenjie; Cen, Jinghe; Liao, Jinqiang; Huang, Jianping; Zhan, Haiying
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1589 - 1592
反应条件
palladium(II) complex with imidazolyl carbene ligandO; caesium acetate in N,N-dimethyl acetamide
T=125°C; 24 h;
参考文献
Toure, B. Barry; Lane, Benjamin S.; Sames, Dalibor
Organic Letters, 2006 , vol. 8, # 10 p. 1979 - 1982
反应条件
sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether
T=75°C; Suzuki cross-coupling reaction; 0.5 h;
参考文献
Enguehard, Cecile; Renou, Jean-Louis; Collot, Valerie; Hervet, Maud; Rault, Sylvain; Gueiffier, Alain
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6572 - 6575
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide
T=120°C; 48 h;
参考文献
Liu, Guoping; Cong, Xuefeng; He, Jiaheng; Luo, Shunzhong; Wu, Di; Lan, Jingbo
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 687 - 690
反应条件
1: 2-aminopyridine With potassium carbonate in o-di-fluorobenzene
0.75 h;
2: phenyl(phenylethynyl)iodonium triflate in o-di-fluorobenzene
T=20°C; DarknessInert atmosphere; regioselective reaction;
参考文献
Dixon, Luke I.; Carroll, Michael A.; Gregson, Thomas J.; Ellames, George J.; Harrington, Ross W.; Clegg, William
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5877 - 5884
反应条件
C26H22Cl2FN3OPd; potassium acetate in N,N-dimethyl acetamide
T=140°C; Heck Reaction; 18 h; Schlenk techniqueInert atmosphere; Reagent/catalyst;
参考文献
Ke, Chun-Hung; Kuo, Bing-Chiuan; Nandi, Debkumar; Lee, Hon Man
Organometallics, 2013 , vol. 32, # 17 p. 4775 - 4784
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide
T=120°C; 24 h;
参考文献
Wu, Zhiqing; Pan, Yinyin; Zhou, Xiangge
Synthesis, 2011 , # 14 art. no. C42011SS, p. 2255 - 2260
反应条件
C46H48N6O5Pd; potassium acetate in N,N-dimethyl acetamide
T=160°C; 24 h; Inert atmosphere;
参考文献
Nandi, Debkumar; Jhou, Yang-Ming; Lee, Jhen-Yi; Kuo, Bing-Chiuan; Liu, Chien-Yu; Huang, Pei-Wen; Lee, Hon Man
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9384 - 9390
反应条件
potassium fluoride in N,N-dimethyl-formamide
T=130°C; 12 h; Inert atmosphere; Reagent/catalystConcentrationSolventTemperatureTime; regioselective reaction;
参考文献
Liu, Guoping; Cong, Xuefeng; He, Jiaheng; Luo, Shunzhong; Wu, Di; Lan, Jingbo
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 687 - 690
