3-甲基-5-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苯甲酸甲酯合成路线 (共 4 条)
反应条件
pinacol borane; 4,4'-di-tert-butylbipyridine in cyclohexane T=80°C;
参考文献
Boebel, Timothy A.; Hartwig, John F.
Tetrahedron, 2008 , vol. 64, # 29 p. 6824 - 6830
反应条件
copper(ll) bromide in methanol T=80°C;
参考文献
Journal of the American Chemical Society, , vol. 129, # 50 p. 15434 - 15435
反应条件
1: With sodium periodate in tetrahydrofuran; water
0.25 h;
2: With hydrogenchloride in tetrahydrofuran; water
4 h;
参考文献
Murphy, Jaclyn M.; Tzschucke, C. Christoph; Hartwig, John F.
Organic Letters, 2007 , vol. 9, # 5 p. 757 - 760
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water
T=80°C; 1 h; High pressure;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143