3,4-O-异亚丙基-L-苏糖酸甲酯合成路线 （共 18 条）
反应条件
in acetonitrile T=80°C; 3 h;
参考文献
Zanardi, Franca; Curti, Claudio; Sartori, Andrea; Rassu, Gloria; Roggio, Annamaria; Battistini, Lucia; Burreddu, Paola; Pinna, Luigi; Pelosi, Giorgio; Casiraghi, Giovanni
European Journal of Organic Chemistry, 2008 , # 13 p. 2273 - 2287
反应条件
sodium hydrogencarbonate; sodium hydroxide in 1-methyl-pyrrolidin-2-one; water T=30 - 60°C; 2 h; Industry scale;
参考文献
US2012/15927 A1, ;
Page/Page column 8-9 ;
反应条件
oxygen; rose bengal in acetone T=-70°C; 4 h; Irradiation;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.; Khan, Saeed I.
Journal of the American Chemical Society, 1989 , vol. 111, # 5 p. 1854 - 1860
反应条件
1: 5,6-O-isopropylidene-L-ascorbic acid With sodium hydroxide; dihydrogen peroxide; sodium hydrogencarbonate in water T=20°C; 1 h; 2: dimethyl sulfate With sodium hydrogencarbonate; sodium sulfite in water T=40°C; 4 h;
参考文献
Cho, Bong Hwan; Kim, Jin Hwan; Jeon, Heung Bae; Kim, Kwan Soo
Tetrahedron, 2005 , vol. 61, # 18 p. 4341 - 4346
反应条件
sodium carbonate in N,N-dimethyl acetamide T=40°C; 6 h;
参考文献
Wei; De Bernardo; Tengi; et al.
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3462 - 3467
反应条件
sodium carbonate in N,N-dimethyl acetamide 48 h; Ambient temperature;
参考文献
Wei; De Bernardo; Tengi; et al.
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3462 - 3467
反应条件
hydrogenchloride; acetic acid in methanol
参考文献
Irie; Igarashi; Matsumoto; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1313 - 1315
反应条件
sodium hydrogencarbonate in water T=40°C; 6 h;
参考文献
Saikia, Bishwajit; Devi, Thongam Joymati; Barua, Nabin C.
Tetrahedron, 2013 , vol. 69, # 9 p. 2157 - 2166
反应条件
1: H2O2; K2CO3 / H2O 2: 93 percent / acetonitrile / 82 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 2 p. 213 - 216
反应条件
1: 85 percent / KMnO4, K2CO3 / H2O / 1) 0 deg C, 30 min., 2) 50 deg C, 2 h 2: 63 percent / HCl, HOAc / methanol View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 6 p. 1451 - 1461
