反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.0833333 h;
2: With N,N'-dimethyl-N,N'-propyleneurea in tetrahydrofuran; hexane
T=-78 - 20°C;
3: 2-(3-iodopropyloxy)-3,4,5,6-tetrahydropyran in tetrahydrofuran; hexane
T=20°C;
参考文献
Gorske, Benjamin C.; Mbofana, Curren T.; Miller, Scott J.
Organic Letters, 2009 , vol. 11, # 19 p. 4318 - 4321