2,5-二甲氧基苯甲醛合成路线 （共 179 条）
参考文献
Journal of the Chemical Society, , vol. 127, p. 2003
反应条件
selenium(IV) oxide; dihydrogen peroxide in tetrahydrofuran 24 h; Heating;
参考文献
Synthetic Communications, , vol. 30, # 24 p. 4425 - 4434
反应条件
1: tin(IV) chloride; bromine / dichloromethane / 20 °C / |Inert atmosphere; |Reflux 2: borane dimethyl sulfide complex / chlorobenzene / 21 h / 0 - 130 °C / |Inert atmosphere View Scheme
参考文献
Bedford, Robin B.; Bowen, John G.; Weeks, Amanda L.
Tetrahedron, 2013 , vol. 69, # 22 p. 4389 - 4394
反应条件
1.1: 73 percent / H2O / 2 h / 75 °C 2.1: N-methylmorpholine-N-oxide; PhSiH3 / Mo(CO)6 / tetrahydrofuran / 16 h / 80 °C 2.2: 76 percent / H2O / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Frost, Christopher G.; Hartley, Benjamin C.
Organic Letters, 2007 , vol. 9, # 21 p. 4259 - 4261
反应条件
1: 97 percent / BBr3 / CH2Cl2 / 1 h / -78 - 0 °C 2: Br2 / CHCl3 / 20 °C 3: 10.64 g / imidazole / CH2Cl2 / 0.25 h / 20 °C View Scheme
参考文献
Li, Chaomin; Johnson, Richard P.; Porco Jr., John A.
Journal of the American Chemical Society, 2003 , vol. 125, # 17 p. 5095 - 5106
反应条件
lithium perchlorate 0.0194444 h; Irradiation;
参考文献
Bandgar; Uppalla; Sadavarte
Journal of Chemical Research - Part S, 2002 , # 1 p. 40 - 41
反应条件
1: 95 percent / dimethylformamide / 12 h / Ambient temperature 2: 86 percent / conc. H2SO4 / 2 h / Ambient temperature View Scheme
参考文献
Armstrong, Veronica; Soto, Oriana; Valderrama, Jaime A.; Tapia, Ricardo
Synthetic Communications, 1988 , vol. 18, # 7 p. 717 - 726
参考文献
Tang, Jing; Huang, Xian
Journal of Chemical Research - Part S, 2003 , # 6 p. 354 - 355
反应条件
1: 76 percent / NaOAc; Ac2O / 8 h / 100 °C 2: 40 percent / aq. HCl / 4 h / 100 °C 3: 11 percent / boron tribromide / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Bailly, Fabrice; Maurin, Cedric; Teissier, Elisabeth; Vezin, Herve; Cotelle, Philippe
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 21 p. 5611 - 5618
反应条件
hydroxylamine hydrochloride in ethanol; water T=70°C; Condensation; 2 h;
参考文献
Illescas, Beatriz M.; Martin, Nazario
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 5986 - 5995
