2,5-二甲氧基苯甲醛合成路线 (共 179 条)
反应条件
sodium acetate; acetic anhydride Kochen des entstandenen 2-Phenyl-4-<2.5-dimethoxy-benzyliden>-oxazolon-(5) mit rotem Phosphor und Jodwasserstoffsaeure in Eisessig;
参考文献
Neuberger
Biochemical Journal, 1948 , vol. 43, p. 599,602
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Bahner,C.T. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 390 - 392
反应条件
(i) KOtBu, (ii) /BRN= 3595639/, Ac2O; Multistep reaction;
参考文献
Harper,S.H. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , vol. <C>, p. 626 - 636
参考文献
Dubuffet; Loutz; Lavielle
Synthetic Communications, 1999 , vol. 29, # 6 p. 929 - 936
反应条件
1: HNO3 / CH2Cl2 / 1 h / 0 - 5 °C 2: AcOH; NaOAc / 5 h / Heating 3: H2; HCOONH4 / Pd/C / ethanol / 0.5 h / Heating View Scheme
参考文献
Catrycke, Marc-Olivier; Houssin, Raymond; Henichart, Jean-Pierre; Pfeiffer, Bruno; Renard, Pierre; Dassonneville, Laurent; Bailly, Christian
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 14 p. 2025 - 2030
参考文献
Billman; Koehler; May
Journal of pharmaceutical sciences, 1969 , vol. 58, # 6 p. 767 - 769
反应条件
bis(2-phenyltrifluoromethanesulfonate)diselenide; dihydrogen peroxide in dichloromethane T=20°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 46, # 50 p. 8665 - 8668
反应条件
selenium(IV) oxide; dihydrogen peroxide in tetrahydrofuran 24 h; Heating;
参考文献
Synthetic Communications, , vol. 30, # 24 p. 4425 - 4434
反应条件
bromine; acetic acid in water T=20°C; 12 h; regiospecific reaction;
参考文献
Koo, Ja Young; Oh, Sangmi; Cho, Seung-Rye; Koh, Minseob; Oh, Won-Keun; Choi, Hueng-Sik; Park, Seung Bum
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5782 - 5786
反应条件
in acetic acid T=20°C; Bromination; 72 h;
参考文献
Organic Preparations and Procedures International, , vol. 23, # 4 p. 419 - 424