2,5-二甲氧基苯甲醛合成路线 （共 179 条）
反应条件
1: 1.3 g / various solvent(s) / 20 h / 160 °C 2: 250 mg / Cu-bronz / quinoline / 7 h / 240 - 260 °C View Scheme
参考文献
Juneja, R. K.; Sharma, S. C.; Tandon, J. S.
Phytochemistry (Elsevier), 1985 , vol. 24, # 2 p. 321 - 324
反应条件
1: 97 percent / BBr3 / CH2Cl2 / 1 h / -78 - 0 °C 2: Br2 / CHCl3 / 20 °C View Scheme
参考文献
Li, Chaomin; Johnson, Richard P.; Porco Jr., John A.
Journal of the American Chemical Society, 2003 , vol. 125, # 17 p. 5095 - 5106
反应条件
potassium permanganate in water T=80°C; 1 h;
参考文献
Azadi-Ardakani, Manouchehr; Wallace, Timothy W.
Tetrahedron, 1988 , vol. 44, # 18 p. 5939 - 5952
反应条件
selenium(IV) oxide; dihydrogen peroxide in tetrahydrofuran 24 h; Heating;
参考文献
Brzaszcz; Kloc; Maposah; Mlochowski
Synthetic Communications, 2000 , vol. 30, # 24 p. 4425 - 4434
反应条件
potassium hydroxide single-cell vs. double-cell electrolysis on Pt-gauze vs. reticulated vitreous carbon anode; Product distribution;
参考文献
Henton, Daniel R.; McCreery, Richard L.; Swenton, John S.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 369 - 378
反应条件
beryllium(II) chloride in toluene 7 h;
参考文献
Sharghi, Hashem; Tamaddon, Fatemeh
Tetrahedron, 1996 , vol. 52, # 43 p. 13623 - 13640
反应条件
1.1: piperidinium acetate / ethanol / 0.5 h 1.2: 57 percent / NaBH3CN / ethanol / 0 - 20 °C 2.1: 32 percent / Sc(OTf)3 / nitromethane / 0.33 h / 100 °C View Scheme
参考文献
SUNSHINE LAKE PHARMA CO.,LTD.; ZHANG, Jiancun; ZHANG, Yingjun; XIE, Hongming; REN, Qingyun; HU, Bailin; FU, Changping; WU, Xiwei; LI, Shifeng; WANG, Chenglin; ZHANG, Zhikeng
Patent: WO2014/82379 A1, 2014 ;
反应条件
water beim Hydrieren des Reaktionsprodukts an Palladium/Kohle in Aethanol;
参考文献
Sterling Drug Inc.
Patent: US2862966 , 1955 ;
反应条件
oxygen; copper; ammonium chloride in pyridine T=60°C; 24 h;
参考文献
Synthesis, , # 6 p. 451 - 452
反应条件
1: 85 percent / piperidine; pyridine 2: 55 percent / PBr3 / CH2Cl2 View Scheme
参考文献
Dubuffet; Loutz; Lavielle
Synthetic Communications, 1999 , vol. 29, # 6 p. 929 - 936
