hydrogenchloride; thiourea in water; acetone
T=25°C; 12 h; Inert atmosphere;
参考文献
Snyder, Scott A.; Breazzano, Steven P.; Ross, Audrey G.; Lin, Yunqing; Zografos, Alexandras L.
Journal of the American Chemical Society, 2009 , vol. 131, p. 1753 - 1765
1.1: 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; oxygen; nitric acid; hydrogenchloride / water; acetonitrile / 24 h / 45 °C / |High pressure; |Sealed tube
2.1: lithium diisopropyl amide / tetrahydrofuran
2.2: -78 - 20 °C
3.1: sodium tetrahydroborate / tetrahydrofuran; water
4.1: 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; nitric acid; sodium nitrite / water; acetic acid / 12 h / 20 °C / 760.05 Torr
View Scheme
参考文献
Rahimi, Alireza; Azarpira, Ali; Kim, Hoon; Ralph, John; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 17 p. 6415 - 6418
