3,4-二甲氧基苯甲酸合成路线 (共 364 条)
反应条件
tert.-butylhydroperoxide; vanadium pentoxide in water T=100°C; 8 h;
参考文献
Tetrahedron, , vol. 67, # 44 p. 8544 - 8551
反应条件
tert.-butylhydroperoxide; 2-phenyl-1,2-benzisoselenazol-3-(2H)-one in tert-butyl alcohol T=75°C; 120 h;
参考文献
Tetrahedron, , vol. 57, # 48 p. 9743 - 9748
反应条件
tert.-butylhydroperoxide; vanadium pentoxide in water T=100°C; 6 h;
参考文献
Tetrahedron, , vol. 67, # 44 p. 8544 - 8551
反应条件
sodium hydroxide in water T=20°C; 6 h;
参考文献
WO2006/40621 A1, ;
Page/Page column 15 ;
WO 2006/040621 A1
反应条件
sodium hypochlorite; sodium hydroxide in water Haloform Reaction; 2 h; TemperatureConcentration;
参考文献
Organic Process Research and Development, , vol. 3, # 5 p. 341 - 346
反应条件
potassium hydroxide in methanol T=35°C; 1 h;
参考文献
Monatshefte fur Chemie, , vol. 135, # 1 p. 83 - 87
反应条件
1: With potassium hydroxide in methanol Nef reaction; Continuous flow conditions; 2: With potassium permanganate; disodium hydrogenphosphate; water in methanol T=25°C; Nef reaction; 0.166667 h; SonicationContinuous flow conditions; 3: With hydrogenchloride; sodium thiosulfate; sodium chloride in methanol; water; ethyl acetate
参考文献
Organic Letters, , vol. 12, # 16 p. 3618 - 3621
反应条件
[bis(acetoxy)iodo]benzene; oxygen in ethyl acetate T=80°C; P=760.051 Torr; 24 h; chemoselective reaction;
参考文献
Chemical Communications, , vol. 49, # 97 p. 11439 - 11441
反应条件
anhydrous potassium trimethylsilanolate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; bis(dibenzylideneacetone)-palladium(0) in toluene T=40°C; 0.333333 h;
参考文献
Organic Letters, , vol. 15, # 6 p. 1378 - 1381
反应条件
[bis(acetoxy)iodo]benzene; oxygen in acetonitrile T=100°C; P=760.051 Torr; 24 h; chemoselective reaction;
参考文献
Chemical Communications, , vol. 49, # 97 p. 11439 - 11441