3,4-二甲氧基苯甲酸合成路线 （共 364 条）
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux 3: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 4: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux 5: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 4 p. 781 - 787
参考文献
Justus Liebigs Annalen der Chemie, , vol. 244, p. 72
反应条件
potassium hydroxide; dihydrogen peroxide in ethanol; water 0.25 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Phytochemistry (Elsevier), , vol. 23, # 7 p. 1493 - 1502
反应条件
potassium permanganate in water; acetone 0.5 h; Heating;
参考文献
Tetrahedron, , vol. 41, # 1 p. 209 - 214
反应条件
chromium(VI) oxide; perchloric acid; acetonitrile T=0 - 5°C; 3 h; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 9 p. 1507 - 1512
反应条件
chromium(VI) oxide; perchloric acid; acetonitrile T=0 - 5°C; 3 h; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 9 p. 1507 - 1512
反应条件
1: 0.14 g / diethyl ether / 48 h 2: 25 mg / KMnO4 / acetone; H2O / 0.5 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 41, # 1 p. 209 - 214
反应条件
1.1: sodium tetrahydroborate / tetrahydrofuran; water 2.1: 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; oxygen / water; acetonitrile / |Sealed tube 2.2: 9 h / 45 °C 3.1: sodium hydroxide; dihydrogen peroxide / tetrahydrofuran; methanol / 10 h / 50 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 17 p. 6415 - 6418
反应条件
1: sodium hydroxide 2: sodium hydroxide; sodium hypochlorite / water / 2 h View Scheme
参考文献
Organic Process Research and Development, , vol. 3, # 5 p. 341 - 346
反应条件
potassium permanganate in acetone
参考文献
Phytochemistry (Elsevier), , vol. 22, # 11 p. 2625 - 2626
