3,4-二甲氧基苯甲酸合成路线 (共 364 条)
反应条件
sodium perchlorate in acetonitrile anode potential 1.0 - 1.1 V;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 833 - 837
反应条件
dihydrogen peroxide; acetic acid; methyltrioxorhenium(VII) on poly(4-vinylpyridine) T=20°C; 6 h; Product distribution; Further Variations:Catalysts;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 15 p. 5292 - 5302
反应条件
water; sodium hydroxide T=60°C; 0.833333 h;
参考文献
Helvetica Chimica Acta, , vol. 95, # 4 p. 586 - 593
反应条件
water; sodium hydroxide T=60°C; 0.833333 h;
参考文献
Helvetica Chimica Acta, , vol. 95, # 4 p. 586 - 593
反应条件
VAZO-52 in acetonitrile T=37°C; 33 h; oxygen saturated solvent; Product distribution;
参考文献
Biochemical Pharmacology, , vol. 52, # 4 p. 519 - 525
反应条件
potassium hydroxide T=70 - 80°C; bei der elektrolytischen Oxydation;
参考文献
Helvetica Chimica Acta, , vol. 8, p. 333
反应条件
oxygen; anhydrous cobalt diacetate; acetic acid T=170°C; P=25857.4 Torr; 3 h; var. reaction partner systems; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1673 - 1679
反应条件
lithium diisopropyl amide 1.) THF, hexane, -70 deg C, 10 min, 2.) THF, hexane, -70 deg C -> room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2451 - 2455
反应条件
2-(2-methoxyphenyl)acetonitrile; lithium diisopropyl amide 1.) THF, hexane, -70 deg C, 10 min; other reagent: LDA/phenylacetonitrile, 2.) THF, hexane, -70 deg C -> room temperature; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2451 - 2455
反应条件
lithium diisopropyl amide 1.) THF, hexane, -70 deg C, 10 min, 2.) THF, hexane, -70 deg C -> room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2451 - 2455