(3,4-二甲氧苯基)乙腈合成路线 （共 124 条）
参考文献
Journal of the American Chemical Society, , vol. 64, p. 885
Journal of the American Chemical Society, , vol. 57, p. 1126
反应条件
sodium hydroxide in water T=80 - 90°C; 2 h; Yield given;
参考文献
Chemistry Letters, , p. 193 - 194
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 2 h; Ambient temperature; Yield given;
参考文献
Synthetic Communications, , vol. 14, # 14 p. 1365 - 1372
反应条件
in ethylene glycol dimethyl ether 24 h; Heating;
参考文献
Fresneda, P. M.; Lidon, M. J.; Molina, P.; Vilaplana, M. J.
Synthesis, 1981 , # 9 p. 711 - 714
参考文献
Vinogradova, V. I.; Yunusov, M. S.; Kuchin, A. V.; Tolstikov, G. A.; Sagandykov, R. T.; et al.
Chemistry of Natural Compounds, 1990 , vol. 26, # 1 p. 54 - 59
Khimiya Prirodnykh Soedinenii, 1990 , # 1 p. 67 - 74
反应条件
1: 1.) NaOEt / 1.) EtOH, 2.) reflux, 2 h 2: 100 percent / NaBH4 / H2O; ethanol / 1 h / 20 - 25 °C 3: 97 percent / SOCl2, pyridine / diethyl ether / 0.5 h / below 5 deg C 4: 92 percent / KI, urea / acetone / 6 h / Heating 5: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 6: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 839 - 850
反应条件
1: 97 percent / SOCl2, pyridine / diethyl ether / 0.5 h / below 5 deg C 2: 92 percent / KI, urea / acetone / 6 h / Heating 3: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 4: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 839 - 850
反应条件
1: 92 percent / KI, urea / acetone / 6 h / Heating 2: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 3: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 839 - 850
反应条件
1: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 2: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 839 - 850
反应条件
1: 100 percent / NaBH4 / H2O; ethanol / 1 h / 20 - 25 °C 2: 97 percent / SOCl2, pyridine / diethyl ether / 0.5 h / below 5 deg C 3: 92 percent / KI, urea / acetone / 6 h / Heating 4: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 5: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 839 - 850
