反应条件
1: diethyl ether
2: 1)potassium t-butoxide / 1)hexamethylphosphoric triamide,THF -40 deg C to -30 deg C 2)-40 deg C to -30 deg C 30 min;
3: 93.1 percent / aq. NaOH / methanol / 1.5 h / Heating
View Scheme
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Miuchi, Shigekazu; Sugibayashi, Hidenori
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, p. 340 - 345
