2-甲氧基-4-甲基苯酚合成路线 (共 145 条)
反应条件
1: With diphenyl-phosphinic acid; triethylamine in N,N-dimethyl-formamide; toluene Curtius-rearrangement; 3 h; Heating; 2: With water in N,N-dimethyl-formamide; toluene Heating; Further stages.;
参考文献
Mirk, Daniela; Waldvogel, Siegfried R.
Tetrahedron Letters, 2004 , vol. 45, # 42 p. 7911 - 7914
反应条件
hydrogen in N-dodecane T=300°C; P=37503.8 Torr; 4 h; Autoclave;
参考文献
Journal of Catalysis, , vol. 285, # 1 p. 315 - 323
反应条件
sulfuric acid; water T=224.84°C; P=21752.2 Torr; 1.5 h; Inert atmosphereAutoclave;
参考文献
ChemSusChem, , vol. 4, # 3 p. 369 - 378
反应条件
poly(4-vinylpyridine-N-oxide) 2 percent cross-linked; dihydrogen peroxide; methyltrioxorhenium (VII) in ethanol; water T=40°C;
参考文献
Tetrahedron, , vol. 58, # 42 p. 8493 - 8500
反应条件
potassium hydroxide T=150 - 155°C; P=11032.6 Torr;
参考文献
DE723412 , ;
DRP/DRBP Org.Chem.
反应条件
1: With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 2 h; Inert atmosphere; 2: With methanol-d1 in tetrahydrofuran; pentane T=-78 - 20°C; Inert atmosphere;
参考文献
Synlett, , # 13 p. 1957 - 1960
反应条件
1.1: 95 percent / aq. NaOH / ethanol / 72 h / 25 °C 2.1: Et3N; DPPA / toluene; dimethylformamide / 3 h / Heating 2.2: 59 percent / H2O / toluene; dimethylformamide / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 42 p. 7911 - 7914
反应条件
sodium in tetrahydrofuran; ammonia T=1°C; Heatingother reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 23 p. 8069 - 8073
反应条件
potassium hydroxide in diethylene glycol Wolff-Kishner reduction; Heating;
参考文献
Synthetic Communications, , vol. 36, # 15 p. 2183 - 2187
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 1 h / Heating 2: KOH / bis-(2-hydroxy-ethyl) ether / Heating View Scheme
参考文献
Synthetic Communications, , vol. 36, # 15 p. 2183 - 2187