反应条件
phosphorus oxychloride in neat (no solvent) anilide and P-compd. stirring at room temp. for 30 min, Fe-compd. addn.,mixt. stirring at room temp. for 3 d, quenching by pouring onto ice, aq . layer extn. after 2 h with Et2O, org. layer drying (MgSO4), vac. concn.; residue flash column chromy. (SiO2, petrol/E2O 7:3 to 5:5), recrystn. (hot petroleum);
参考文献
Alonso, Francisco; Davies, Stephen G.; Elend, Almut S.; Haggitt, Jane L.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 2 p. 257 - 264
