1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
trichlorophosphate in not given Vilsmeyer formylation;;
参考文献
Rosenblum, M.
Chemistry and Industry (London, United Kingdom), 1957 , p. 72 - 72
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Gmelin Handbook: Fe: Org.Verb.A1, 2.5.7.7, page 161 - 162
1: 4-bromo-2-chloro-1-methoxy-benzene With magnesium in diethyl ether T=0°C; 2: N-methyl-N-formyl-aniline in diethyl ether T=20°C; 3 h;
参考文献
Fujio, Mizue; Umezaki, Yuzo; Alam, Md. Ashadul; Kikukawa, Kiyoshi; Fujiyama, Ryoji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1091 - 1099
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h;
